Patent
Atlas literature
Patent
US 11,946,161 B2Patent drawings and their descriptions. Click a drawing to enlarge it.
FIGS. 1A-1C are scanning electron microscope micro- graphs of Ni₂Mo₆S₆O₂/MoS₂ at three different scales;
FIG. 2 is an atomic force microscope micrograph of 60 Ni₂Mo₆S₆O₂/MoS2;
FIG. 3 is an X-ray diffraction fast-scan (with a scanning speed of 10°/min) spectrum of Ni₂Mo₆S₆O₂/MoS2;
FIG. 4 is an X-ray diffraction fast-scan (with a scanning speed of 0.1°/min) spectrum of Ni₂Mo₆S₆O/MoS2; 65
FIG. 5 is an electron diffraction spectrum of a selected area of Ni₂Mo₆S₆O₂/MoS2; B₂
FIG. 6 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS2, NiS₂ and MoS2;
FIG. 7 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS₂ and PVC (20%); and
FIG. 8 is a graph of multi-step constant current of Ni₂Mo₆S₆O₂/MoS₂ and Pt/C (20%.
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
A method for synthesizing an intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet with exposed (00L) crystal planes, comprising: using an ion insertion method to restrict Ni ions to be located in a lattice matrix of a Mo-based compound to form an Ni—Mo bonded precursor; adjusting and controlling a concentration of a sulfur atmosphere to form a dinuclear metal sulfide Ni₂Mo₆S₆O₂ and using a method for growing a single crystal in a limited area to adjust and control a growth direction of Ni₂Mo₆S₆O2, wherein the Ni₂Mo₆S₆O₂ is grown, and a single crystal MoS₂ is used as a growth template, with the single crystal MoS₂ alternately along a crystal plane (110) of the single crystal MoS2, to form a twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet, wherein the Ni₂Mo₆S₆O₂ and the MoS₂ are intergrown in the twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
The method according to claim 1, comprising the steps of:
A method of electrocatalytic water decomposition in a hydrogen evolution reaction, comprising the step of using the intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet with the exposed (00L) crystal planes obtained by the method according to claim 1 as a catalyst in the elec-trocatalytic water decomposition in the hydrogen evolution reaction.
Obtaining a second mixture, by mixing and stirring the first solution, the second solution, and all the undis-solved soluble salt solids of step 2);
Obtaining a dry solid, by placing the second mixture in liquid nitrogen for freezing and then placing the second mixture in a vacuum freeze dryer for vacuum freeze-drying for 12-48 hours, wherein the dry solid obtained is placed in a first porcelain boat, and then the first porcelain boat is placed in a center of a tube furnace, and a second porcelain boat containing a sulfur source is placed at an uptake port of the first porcelain boat, and a distance between the first porcelain boat and the second porcelain boat is precisely adjusted to be 3-4 cm;
Introducing inert gas into the tube furnace, adjusting and controlling a flow rate of the inert gas to be 10-25 mL/min, and raising a temperature to a target tempera-ture for constant temperature calcination; wherein a temperature raising rate is 1-10° C./min, the target temperature is 300-500° C., and a constant temperature calcination time is 1-10 hours; and
Taking out the first porcelain boat after a vulcanization is completed, and washing a sample in the first porce-lain boat with pure water and ethanol and then drying at room temperature, wherein a resulting product is the intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
Embodiments described in the patent, grouped by the materials and process steps they use.
5 materials1 process step
Synthesis of intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet: (1) A molybdenum source and nickel source at Mo:Ni molar ratio 1:1.5 are dissolved in 5 wt% H₂O₂ aqueous solution at 60°C to form solution A. (2) 20 g of soluble salt is added to 15 mL pure water, heated to 60°C with stirring until crystallization occurs, then cooled in ice water to yield saturated solution B with undissolved solids. (3) 0.1 mL of solution A and 1 mL of solution B plus all undissolved solids are mixed to form mixture C. (4) Mixture C is frozen in liquid nitrogen, then vacuum freeze-dried for 24 hours; resulting dry solid is placed in porcelain boat A at the center of a tube furnace, with porcelain boat B containing 20 g sulfur source placed at uptake port at a precisely adjusted distance of 3.5 cm. (5) Inert gas is introduced at 15 mL/min, temperature raised to 400°C at 5°C/min, and held for 5 hours. (6) After vulcanization, sample is washed with pure water and ethanol and dried at room temperature to yield intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
Materials described outside the worked examples.
molybdenum source
nickel source
Measurements and analyses referenced in the patent, with their drawing references.
FIGS. 1A-1C are scanning electron microscope micro- graphs of Ni₂Mo₆S₆O₂/MoS₂ at three different scales;
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Temperature | 60–90 °C | — |
Temperature | 60–100 °C |
Patents and literature cited by this patent (applicant and examiner references).
Cited patents · 10
Related documents with shared materials, methods, properties, or citations.
Patent
Atlas literature
Patent
US 11,946,161 B2Patent drawings and their descriptions. Click a drawing to enlarge it.
FIGS. 1A-1C are scanning electron microscope micro- graphs of Ni₂Mo₆S₆O₂/MoS₂ at three different scales;
FIG. 2 is an atomic force microscope micrograph of 60 Ni₂Mo₆S₆O₂/MoS2;
FIG. 3 is an X-ray diffraction fast-scan (with a scanning speed of 10°/min) spectrum of Ni₂Mo₆S₆O₂/MoS2;
FIG. 4 is an X-ray diffraction fast-scan (with a scanning speed of 0.1°/min) spectrum of Ni₂Mo₆S₆O/MoS2; 65
FIG. 5 is an electron diffraction spectrum of a selected area of Ni₂Mo₆S₆O₂/MoS2; B₂
FIG. 6 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS2, NiS₂ and MoS2;
FIG. 7 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS₂ and PVC (20%); and
FIG. 8 is a graph of multi-step constant current of Ni₂Mo₆S₆O₂/MoS₂ and Pt/C (20%.
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
A method for synthesizing an intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet with exposed (00L) crystal planes, comprising: using an ion insertion method to restrict Ni ions to be located in a lattice matrix of a Mo-based compound to form an Ni—Mo bonded precursor; adjusting and controlling a concentration of a sulfur atmosphere to form a dinuclear metal sulfide Ni₂Mo₆S₆O₂ and using a method for growing a single crystal in a limited area to adjust and control a growth direction of Ni₂Mo₆S₆O2, wherein the Ni₂Mo₆S₆O₂ is grown, and a single crystal MoS₂ is used as a growth template, with the single crystal MoS₂ alternately along a crystal plane (110) of the single crystal MoS2, to form a twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet, wherein the Ni₂Mo₆S₆O₂ and the MoS₂ are intergrown in the twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
The method according to claim 1, comprising the steps of:
A method of electrocatalytic water decomposition in a hydrogen evolution reaction, comprising the step of using the intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet with the exposed (00L) crystal planes obtained by the method according to claim 1 as a catalyst in the elec-trocatalytic water decomposition in the hydrogen evolution reaction.
Obtaining a second mixture, by mixing and stirring the first solution, the second solution, and all the undis-solved soluble salt solids of step 2);
Obtaining a dry solid, by placing the second mixture in liquid nitrogen for freezing and then placing the second mixture in a vacuum freeze dryer for vacuum freeze-drying for 12-48 hours, wherein the dry solid obtained is placed in a first porcelain boat, and then the first porcelain boat is placed in a center of a tube furnace, and a second porcelain boat containing a sulfur source is placed at an uptake port of the first porcelain boat, and a distance between the first porcelain boat and the second porcelain boat is precisely adjusted to be 3-4 cm;
Introducing inert gas into the tube furnace, adjusting and controlling a flow rate of the inert gas to be 10-25 mL/min, and raising a temperature to a target tempera-ture for constant temperature calcination; wherein a temperature raising rate is 1-10° C./min, the target temperature is 300-500° C., and a constant temperature calcination time is 1-10 hours; and
Taking out the first porcelain boat after a vulcanization is completed, and washing a sample in the first porce-lain boat with pure water and ethanol and then drying at room temperature, wherein a resulting product is the intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
Embodiments described in the patent, grouped by the materials and process steps they use.
5 materials1 process step
Synthesis of intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet: (1) A molybdenum source and nickel source at Mo:Ni molar ratio 1:1.5 are dissolved in 5 wt% H₂O₂ aqueous solution at 60°C to form solution A. (2) 20 g of soluble salt is added to 15 mL pure water, heated to 60°C with stirring until crystallization occurs, then cooled in ice water to yield saturated solution B with undissolved solids. (3) 0.1 mL of solution A and 1 mL of solution B plus all undissolved solids are mixed to form mixture C. (4) Mixture C is frozen in liquid nitrogen, then vacuum freeze-dried for 24 hours; resulting dry solid is placed in porcelain boat A at the center of a tube furnace, with porcelain boat B containing 20 g sulfur source placed at uptake port at a precisely adjusted distance of 3.5 cm. (5) Inert gas is introduced at 15 mL/min, temperature raised to 400°C at 5°C/min, and held for 5 hours. (6) After vulcanization, sample is washed with pure water and ethanol and dried at room temperature to yield intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
Materials described outside the worked examples.
molybdenum source
nickel source
Measurements and analyses referenced in the patent, with their drawing references.
FIGS. 1A-1C are scanning electron microscope micro- graphs of Ni₂Mo₆S₆O₂/MoS₂ at three different scales;
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Temperature | 60–90 °C | — |
Temperature | 60–100 °C |
Patents and literature cited by this patent (applicant and examiner references).
Cited patents · 10
Related documents with shared materials, methods, properties, or citations.
Patent
Atlas literature
Patent
US 11,946,161 B2Patent drawings and their descriptions. Click a drawing to enlarge it.
FIGS. 1A-1C are scanning electron microscope micro- graphs of Ni₂Mo₆S₆O₂/MoS₂ at three different scales;
FIG. 2 is an atomic force microscope micrograph of 60 Ni₂Mo₆S₆O₂/MoS2;
FIG. 3 is an X-ray diffraction fast-scan (with a scanning speed of 10°/min) spectrum of Ni₂Mo₆S₆O₂/MoS2;
FIG. 4 is an X-ray diffraction fast-scan (with a scanning speed of 0.1°/min) spectrum of Ni₂Mo₆S₆O/MoS2; 65
FIG. 5 is an electron diffraction spectrum of a selected area of Ni₂Mo₆S₆O₂/MoS2; B₂
FIG. 6 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS2, NiS₂ and MoS2;
FIG. 7 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS₂ and PVC (20%); and
FIG. 8 is a graph of multi-step constant current of Ni₂Mo₆S₆O₂/MoS₂ and Pt/C (20%.
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
A method for synthesizing an intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet with exposed (00L) crystal planes, comprising: using an ion insertion method to restrict Ni ions to be located in a lattice matrix of a Mo-based compound to form an Ni—Mo bonded precursor; adjusting and controlling a concentration of a sulfur atmosphere to form a dinuclear metal sulfide Ni₂Mo₆S₆O₂ and using a method for growing a single crystal in a limited area to adjust and control a growth direction of Ni₂Mo₆S₆O2, wherein the Ni₂Mo₆S₆O₂ is grown, and a single crystal MoS₂ is used as a growth template, with the single crystal MoS₂ alternately along a crystal plane (110) of the single crystal MoS2, to form a twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet, wherein the Ni₂Mo₆S₆O₂ and the MoS₂ are intergrown in the twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
The method according to claim 1, comprising the steps of:
A method of electrocatalytic water decomposition in a hydrogen evolution reaction, comprising the step of using the intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet with the exposed (00L) crystal planes obtained by the method according to claim 1 as a catalyst in the elec-trocatalytic water decomposition in the hydrogen evolution reaction.
Obtaining a second mixture, by mixing and stirring the first solution, the second solution, and all the undis-solved soluble salt solids of step 2);
Obtaining a dry solid, by placing the second mixture in liquid nitrogen for freezing and then placing the second mixture in a vacuum freeze dryer for vacuum freeze-drying for 12-48 hours, wherein the dry solid obtained is placed in a first porcelain boat, and then the first porcelain boat is placed in a center of a tube furnace, and a second porcelain boat containing a sulfur source is placed at an uptake port of the first porcelain boat, and a distance between the first porcelain boat and the second porcelain boat is precisely adjusted to be 3-4 cm;
Introducing inert gas into the tube furnace, adjusting and controlling a flow rate of the inert gas to be 10-25 mL/min, and raising a temperature to a target tempera-ture for constant temperature calcination; wherein a temperature raising rate is 1-10° C./min, the target temperature is 300-500° C., and a constant temperature calcination time is 1-10 hours; and
Taking out the first porcelain boat after a vulcanization is completed, and washing a sample in the first porce-lain boat with pure water and ethanol and then drying at room temperature, wherein a resulting product is the intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
Embodiments described in the patent, grouped by the materials and process steps they use.
5 materials1 process step
Synthesis of intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet: (1) A molybdenum source and nickel source at Mo:Ni molar ratio 1:1.5 are dissolved in 5 wt% H₂O₂ aqueous solution at 60°C to form solution A. (2) 20 g of soluble salt is added to 15 mL pure water, heated to 60°C with stirring until crystallization occurs, then cooled in ice water to yield saturated solution B with undissolved solids. (3) 0.1 mL of solution A and 1 mL of solution B plus all undissolved solids are mixed to form mixture C. (4) Mixture C is frozen in liquid nitrogen, then vacuum freeze-dried for 24 hours; resulting dry solid is placed in porcelain boat A at the center of a tube furnace, with porcelain boat B containing 20 g sulfur source placed at uptake port at a precisely adjusted distance of 3.5 cm. (5) Inert gas is introduced at 15 mL/min, temperature raised to 400°C at 5°C/min, and held for 5 hours. (6) After vulcanization, sample is washed with pure water and ethanol and dried at room temperature to yield intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
Materials described outside the worked examples.
molybdenum source
nickel source
Measurements and analyses referenced in the patent, with their drawing references.
FIGS. 1A-1C are scanning electron microscope micro- graphs of Ni₂Mo₆S₆O₂/MoS₂ at three different scales;
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Temperature | 60–90 °C | — |
Temperature | 60–100 °C |
Patents and literature cited by this patent (applicant and examiner references).
Cited patents · 10
Related documents with shared materials, methods, properties, or citations.
Patent
Atlas literature
Patent
US 11,946,161 B2Patent drawings and their descriptions. Click a drawing to enlarge it.
FIGS. 1A-1C are scanning electron microscope micro- graphs of Ni₂Mo₆S₆O₂/MoS₂ at three different scales;
FIG. 2 is an atomic force microscope micrograph of 60 Ni₂Mo₆S₆O₂/MoS2;
FIG. 3 is an X-ray diffraction fast-scan (with a scanning speed of 10°/min) spectrum of Ni₂Mo₆S₆O₂/MoS2;
FIG. 4 is an X-ray diffraction fast-scan (with a scanning speed of 0.1°/min) spectrum of Ni₂Mo₆S₆O/MoS2; 65
FIG. 5 is an electron diffraction spectrum of a selected area of Ni₂Mo₆S₆O₂/MoS2; B₂
FIG. 6 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS2, NiS₂ and MoS2;
FIG. 7 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS₂ and PVC (20%); and
FIG. 8 is a graph of multi-step constant current of Ni₂Mo₆S₆O₂/MoS₂ and Pt/C (20%.
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
A method for synthesizing an intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet with exposed (00L) crystal planes, comprising: using an ion insertion method to restrict Ni ions to be located in a lattice matrix of a Mo-based compound to form an Ni—Mo bonded precursor; adjusting and controlling a concentration of a sulfur atmosphere to form a dinuclear metal sulfide Ni₂Mo₆S₆O₂ and using a method for growing a single crystal in a limited area to adjust and control a growth direction of Ni₂Mo₆S₆O2, wherein the Ni₂Mo₆S₆O₂ is grown, and a single crystal MoS₂ is used as a growth template, with the single crystal MoS₂ alternately along a crystal plane (110) of the single crystal MoS2, to form a twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet, wherein the Ni₂Mo₆S₆O₂ and the MoS₂ are intergrown in the twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
The method according to claim 1, comprising the steps of:
A method of electrocatalytic water decomposition in a hydrogen evolution reaction, comprising the step of using the intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet with the exposed (00L) crystal planes obtained by the method according to claim 1 as a catalyst in the elec-trocatalytic water decomposition in the hydrogen evolution reaction.
Obtaining a second mixture, by mixing and stirring the first solution, the second solution, and all the undis-solved soluble salt solids of step 2);
Obtaining a dry solid, by placing the second mixture in liquid nitrogen for freezing and then placing the second mixture in a vacuum freeze dryer for vacuum freeze-drying for 12-48 hours, wherein the dry solid obtained is placed in a first porcelain boat, and then the first porcelain boat is placed in a center of a tube furnace, and a second porcelain boat containing a sulfur source is placed at an uptake port of the first porcelain boat, and a distance between the first porcelain boat and the second porcelain boat is precisely adjusted to be 3-4 cm;
Introducing inert gas into the tube furnace, adjusting and controlling a flow rate of the inert gas to be 10-25 mL/min, and raising a temperature to a target tempera-ture for constant temperature calcination; wherein a temperature raising rate is 1-10° C./min, the target temperature is 300-500° C., and a constant temperature calcination time is 1-10 hours; and
Taking out the first porcelain boat after a vulcanization is completed, and washing a sample in the first porce-lain boat with pure water and ethanol and then drying at room temperature, wherein a resulting product is the intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
Embodiments described in the patent, grouped by the materials and process steps they use.
5 materials1 process step
Synthesis of intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet: (1) A molybdenum source and nickel source at Mo:Ni molar ratio 1:1.5 are dissolved in 5 wt% H₂O₂ aqueous solution at 60°C to form solution A. (2) 20 g of soluble salt is added to 15 mL pure water, heated to 60°C with stirring until crystallization occurs, then cooled in ice water to yield saturated solution B with undissolved solids. (3) 0.1 mL of solution A and 1 mL of solution B plus all undissolved solids are mixed to form mixture C. (4) Mixture C is frozen in liquid nitrogen, then vacuum freeze-dried for 24 hours; resulting dry solid is placed in porcelain boat A at the center of a tube furnace, with porcelain boat B containing 20 g sulfur source placed at uptake port at a precisely adjusted distance of 3.5 cm. (5) Inert gas is introduced at 15 mL/min, temperature raised to 400°C at 5°C/min, and held for 5 hours. (6) After vulcanization, sample is washed with pure water and ethanol and dried at room temperature to yield intergrown twin Ni₂Mo₆S₆O₂/MoS₂ two-dimensional nanosheet.
Materials described outside the worked examples.
molybdenum source
nickel source
Measurements and analyses referenced in the patent, with their drawing references.
FIGS. 1A-1C are scanning electron microscope micro- graphs of Ni₂Mo₆S₆O₂/MoS₂ at three different scales;
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Temperature | 60–90 °C | — |
Temperature | 60–100 °C |
Patents and literature cited by this patent (applicant and examiner references).
Cited patents · 10
Related documents with shared materials, methods, properties, or citations.
Ni-Mo bonded precursor
FIG. 2 is an atomic force microscope micrograph of 60 Ni₂Mo₆S₆O₂/MoS2;
FIG. 3 is an X-ray diffraction fast-scan (with a scanning speed of 10°/min) spectrum of Ni₂Mo₆S₆O₂/MoS2;
FIG. 4 is an X-ray diffraction fast-scan (with a scanning speed of 0.1°/min) spectrum of Ni₂Mo₆S₆O/MoS2; 65
FIG. 5 is an electron diffraction spectrum of a selected area of Ni₂Mo₆S₆O₂/MoS2; B₂
FIG. 6 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS2, NiS₂ and MoS2;
FIG. 7 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS₂ and PVC (20%); and
FIG. 8 is a graph of multi-step constant current of Ni₂Mo₆S₆O₂/MoS₂ and Pt/C (20%.
| — |
Duration | 24–48 hours | — |
Thickness | 3.5–4 cm | — |
Temperature | 5–10 °C | — |
Temperature | 400–500 °C | — |
Duration | 5–10 hours | — |
Duration | 12–48 hours | — |
Thickness | 3–4 cm | — |
Temperature | 1–10 °C | — |
Temperature | 300–500 °C | — |
Duration | 1–10 hours | — |
Temperature | 50–100 °C | — |
Cited non-patent literature · 2
Ni-Mo bonded precursor
FIG. 2 is an atomic force microscope micrograph of 60 Ni₂Mo₆S₆O₂/MoS2;
FIG. 3 is an X-ray diffraction fast-scan (with a scanning speed of 10°/min) spectrum of Ni₂Mo₆S₆O₂/MoS2;
FIG. 4 is an X-ray diffraction fast-scan (with a scanning speed of 0.1°/min) spectrum of Ni₂Mo₆S₆O/MoS2; 65
FIG. 5 is an electron diffraction spectrum of a selected area of Ni₂Mo₆S₆O₂/MoS2; B₂
FIG. 6 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS2, NiS₂ and MoS2;
FIG. 7 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS₂ and PVC (20%); and
FIG. 8 is a graph of multi-step constant current of Ni₂Mo₆S₆O₂/MoS₂ and Pt/C (20%.
| — |
Duration | 24–48 hours | — |
Thickness | 3.5–4 cm | — |
Temperature | 5–10 °C | — |
Temperature | 400–500 °C | — |
Duration | 5–10 hours | — |
Duration | 12–48 hours | — |
Thickness | 3–4 cm | — |
Temperature | 1–10 °C | — |
Temperature | 300–500 °C | — |
Duration | 1–10 hours | — |
Temperature | 50–100 °C | — |
Cited non-patent literature · 2
Ni-Mo bonded precursor
FIG. 2 is an atomic force microscope micrograph of 60 Ni₂Mo₆S₆O₂/MoS2;
FIG. 3 is an X-ray diffraction fast-scan (with a scanning speed of 10°/min) spectrum of Ni₂Mo₆S₆O₂/MoS2;
FIG. 4 is an X-ray diffraction fast-scan (with a scanning speed of 0.1°/min) spectrum of Ni₂Mo₆S₆O/MoS2; 65
FIG. 5 is an electron diffraction spectrum of a selected area of Ni₂Mo₆S₆O₂/MoS2; B₂
FIG. 6 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS2, NiS₂ and MoS2;
FIG. 7 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS₂ and PVC (20%); and
FIG. 8 is a graph of multi-step constant current of Ni₂Mo₆S₆O₂/MoS₂ and Pt/C (20%.
| — |
Duration | 24–48 hours | — |
Thickness | 3.5–4 cm | — |
Temperature | 5–10 °C | — |
Temperature | 400–500 °C | — |
Duration | 5–10 hours | — |
Duration | 12–48 hours | — |
Thickness | 3–4 cm | — |
Temperature | 1–10 °C | — |
Temperature | 300–500 °C | — |
Duration | 1–10 hours | — |
Temperature | 50–100 °C | — |
Cited non-patent literature · 2
Ni-Mo bonded precursor
FIG. 2 is an atomic force microscope micrograph of 60 Ni₂Mo₆S₆O₂/MoS2;
FIG. 3 is an X-ray diffraction fast-scan (with a scanning speed of 10°/min) spectrum of Ni₂Mo₆S₆O₂/MoS2;
FIG. 4 is an X-ray diffraction fast-scan (with a scanning speed of 0.1°/min) spectrum of Ni₂Mo₆S₆O/MoS2; 65
FIG. 5 is an electron diffraction spectrum of a selected area of Ni₂Mo₆S₆O₂/MoS2; B₂
FIG. 6 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS2, NiS₂ and MoS2;
FIG. 7 is a graph of linear scanning for Ni₂Mo₆S₆O₂/MoS₂ and PVC (20%); and
FIG. 8 is a graph of multi-step constant current of Ni₂Mo₆S₆O₂/MoS₂ and Pt/C (20%.
| — |
Duration | 24–48 hours | — |
Thickness | 3.5–4 cm | — |
Temperature | 5–10 °C | — |
Temperature | 400–500 °C | — |
Duration | 5–10 hours | — |
Duration | 12–48 hours | — |
Thickness | 3–4 cm | — |
Temperature | 1–10 °C | — |
Temperature | 300–500 °C | — |
Duration | 1–10 hours | — |
Temperature | 50–100 °C | — |
Cited non-patent literature · 2
