Patent
US 9,449,787LIQUID FLOW CELLS HAVING GRAPHENE ON NITRIDE FOR MICROSCOPY
Vivekananda P. Adiga, Gabriel Dunn, Alexander K. Zettl, A. Paul Alivisatos
US
Copyright © 2026 Matter42. All rights reserved.
Patent
Atlas literature
Patent
US 9,449,787Patent drawings and their descriptions. Click a drawing to enlarge it.
Figure 1 shows an example of a flow diagram illustrating a manufacturing process for a liquid flow cell.
Figures 2A-2 I show examples of schematic illustrations of a liquid flow cell at various stages in the manufacturing process.
Figure 2J shows an example of a cross-sectional schematic illustration of a liquid flow cell.
Figure 3 shows an example of a flow diagram illustrating a manufacturing process for a liquid flow cell having a top plate.
Figures 4A-4G show examples of schematic illustrations of a liquid flow cell having a top plate at various stages in the manufacturing process.
Figure 5 shows an example of a top-down schematic illustration of a liquid flow cell including electrodes.
Figure 6 shows an example of a cross-sectional schematic illustration of a liquid flow cell including two graphene sheets.
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
A device comprising: a first plate, the first plate comprising: a first substrate, the first substrate having a first surface and a second surface; a first oxide layer disposed on the first surface of the first substrate and a second oxide layer disposed on the second surface of the first substrate; a first nitride layer disposed on the first oxide layer and a second nitride layer disposed on the second oxide layer; a cavity defined in the first oxide layer, the first nitride layer, and the first substrate, the cavity including a third nitride layer disposed on walls of the first substrate and the second oxide layer that define the cavity; a channel defined in the second oxide layer; an inlet port and an outlet port defined in the second nitride layer in fluid communication with the channel; a plurality of viewports defined in the second nitride layer positioned between the inlet port and the outlet port, at least some of the plurality of viewports positioned opposite the cavity; and a first graphene sheet disposed on the second nitride layer covering the plurality of viewports.
The device of claim 1, further comprising: a second plate, the second plate comprising: a second substrate having a first surface and a second surface; a third oxide layer disposed on the first surface of the second substrate and a fourth oxide layer disposed on the second surface of the second substrate; and a third nitride layer disposed on the third oxide layer and a fourth nitride layer disposed on the fourth oxide layer, wherein the second plate defines a through hole Attorney Docket No.: 2014-129-02 through the third nitride layer, the third oxide layer, the second substrate, the fourth oxide layer, and the fourth nitride layer; and a polymer material joining the graphene sheet of the first plate and the fourth nitride layer of the second plate, wherein the first and the second plates are joined so that the cavity of the first plate is aligned with the though hole in the second plate.
The device of claim 1, wherein first substrate comprises silicon, wherein the first and second oxide layers comprise silicon oxide, and wherein the first, second, and third nitride layers comprise silicon nitride.
The device of claim 1, wherein the graphene sheet comprises a few layers of graphene.
The device of claim 1, wherein the inlet port, the outlet port, and the plurality of view ports are about 60 nanometers to 500 nanometers in diameter.
The device of claim 1, wherein the first substrate is about 150 microns to 450 microns thick.
The device of claim 1, wherein the first surface and the second surface have dimensions of about 2 millimeters to 8 millimeters by about 2 millimeters to 8 millimeters. 21 Attorney Docket No.: 2014-129-02
The device of claim 1, further comprising: a first electrode disposed on the second nitride layer, wherein the first electrode comp ri ses: a first contact pad proximate an edge of the second nitride layer, a first probe at an edge of the inlet port, and a first lead connecting the first contact pad and the first probe; and a second electrode disposed on the second nitride layer, wherein the second electrode comp ri ses: a second contact pad proximate the edge of the second nitride layer, a second probe at an edge of the outlet port, and a second lead connecting the second contact pad and the second probe.
The device of claim 1, wherein a second plurality of viewports is defined in the third nitride layer, further comprising: a second graphene sheet disposed on the third nitride layer covering the second plurality of viewports.
A device comprising: a first substrate, the first substrate having a first surface and a second surface; a first nitride layer disposed on the first surface of the first substrate and a second nitride layer disposed on the second surface of the first substrate; an oxide layer disposed on the second nitride layer; a third nitride layer disposed on the oxide layer; a cavity defined in the first nitride layer and the first substrate; a channel defined in the oxide layer; an inlet port and an outlet port defined in the third nitride layer in fluid communication with the channel; 22 Attorney Docket No.: 2014-129-02 a plurality of viewports defined in the third nitride layer positioned between the inlet port and the outlet port, at least some of the plurality of viewports positioned opposite the cavity; and a first graphene sheet disposed on the third nitride layer covering the plurality of viewports.
A method comprising: (a) forming a first oxide layer on a first surface of a first substrate and a second oxide layer on a second surface of the first substrate; (b) depositing a first nitride layer on the first oxide layer and a second nitride layer on the second oxide layer; (c) removing a portion of the first nitride layer and the first oxide layer; (d) forming a cavity in the first substrate to expose the second oxide layer; (e) depositing a third nitride layer on the first nitride layer, first substrate walls of the cavity, and the second oxide layer; (f) forming an inlet port, an outlet port, and a plurality of viewports between the inlet port and the outlet port in the second nitride layer, at least some of the plurality of viewports positioned to be opposite the cavity; (g) removing a portion of the second oxide layer to form a channel from the inlet port to the outlet port; and (h) positioning a graphene sheet on the second nitride layer to cover the plurality of viewports.
The method of claim 16, further comprising: forming a first oxide layer on a first surface of a second substrate and a second oxide layer on a second surface of the second substrate; depositing a first nitride layer on the first oxide layer of the second substrate and a second nitride layer on the second oxide layer of the second substrate; removing a portion of the first nitride layer and the first oxide layer of the second substrate; forming a cavity in the second substrate to expose the second oxide layer of the second substrate; 23 Attorney Docket No.: 2014-129-02 depositing a polymer material on the second nitride layer of the second substrate; removing a portion of the polymer material, the second nitride layer of the second substrate, and the second oxide layer of the second substrate to form a through hole; and joining the graphene sheet of the first substrate to the second nitride layer of the second substrate with the polymer material, wherein the cavity of the first substrate is aligned with the though hole of the second substrate.
The method of claim 16, further comprising: after operation (e), forming a first electrode on the second nitride layer, wherein the first electrode includes a first contact pad proximate an edge of the second nitride layer, a first probe at an edge of the inlet port, and a first lead connecting the first contact pad and the first probe; and forming a second electrode on the second nitride layer, wherein the second electrode includes a second contact pad proximate the edge of the second nitride layer, a second probe at an edge of the outlet port, and a second lead connecting the second contact pad and the second probe.
The method of claim 16, wherein operation (f) includes forming a second plurality of viewports in the third nitride layer.
Layer stacks claimed or described, ordered top of device to substrate.
liquid flow cell (graphene on nitride, two-plate)
Materials described outside the worked examples.
graphene
substrate
Additional fabrication and treatment steps described in the patent.
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Thickness | 60–500 nm | — |
Thickness |
Related documents with shared materials, methods, properties, or citations.
Patent
Atlas literature
Patent
US 9,449,787Patent drawings and their descriptions. Click a drawing to enlarge it.
Figure 1 shows an example of a flow diagram illustrating a manufacturing process for a liquid flow cell.
Figures 2A-2 I show examples of schematic illustrations of a liquid flow cell at various stages in the manufacturing process.
Figure 2J shows an example of a cross-sectional schematic illustration of a liquid flow cell.
Figure 3 shows an example of a flow diagram illustrating a manufacturing process for a liquid flow cell having a top plate.
Figures 4A-4G show examples of schematic illustrations of a liquid flow cell having a top plate at various stages in the manufacturing process.
Figure 5 shows an example of a top-down schematic illustration of a liquid flow cell including electrodes.
Figure 6 shows an example of a cross-sectional schematic illustration of a liquid flow cell including two graphene sheets.
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
A device comprising: a first plate, the first plate comprising: a first substrate, the first substrate having a first surface and a second surface; a first oxide layer disposed on the first surface of the first substrate and a second oxide layer disposed on the second surface of the first substrate; a first nitride layer disposed on the first oxide layer and a second nitride layer disposed on the second oxide layer; a cavity defined in the first oxide layer, the first nitride layer, and the first substrate, the cavity including a third nitride layer disposed on walls of the first substrate and the second oxide layer that define the cavity; a channel defined in the second oxide layer; an inlet port and an outlet port defined in the second nitride layer in fluid communication with the channel; a plurality of viewports defined in the second nitride layer positioned between the inlet port and the outlet port, at least some of the plurality of viewports positioned opposite the cavity; and a first graphene sheet disposed on the second nitride layer covering the plurality of viewports.
The device of claim 1, further comprising: a second plate, the second plate comprising: a second substrate having a first surface and a second surface; a third oxide layer disposed on the first surface of the second substrate and a fourth oxide layer disposed on the second surface of the second substrate; and a third nitride layer disposed on the third oxide layer and a fourth nitride layer disposed on the fourth oxide layer, wherein the second plate defines a through hole Attorney Docket No.: 2014-129-02 through the third nitride layer, the third oxide layer, the second substrate, the fourth oxide layer, and the fourth nitride layer; and a polymer material joining the graphene sheet of the first plate and the fourth nitride layer of the second plate, wherein the first and the second plates are joined so that the cavity of the first plate is aligned with the though hole in the second plate.
The device of claim 1, wherein first substrate comprises silicon, wherein the first and second oxide layers comprise silicon oxide, and wherein the first, second, and third nitride layers comprise silicon nitride.
The device of claim 1, wherein the graphene sheet comprises a few layers of graphene.
The device of claim 1, wherein the inlet port, the outlet port, and the plurality of view ports are about 60 nanometers to 500 nanometers in diameter.
The device of claim 1, wherein the first substrate is about 150 microns to 450 microns thick.
The device of claim 1, wherein the first surface and the second surface have dimensions of about 2 millimeters to 8 millimeters by about 2 millimeters to 8 millimeters. 21 Attorney Docket No.: 2014-129-02
The device of claim 1, further comprising: a first electrode disposed on the second nitride layer, wherein the first electrode comp ri ses: a first contact pad proximate an edge of the second nitride layer, a first probe at an edge of the inlet port, and a first lead connecting the first contact pad and the first probe; and a second electrode disposed on the second nitride layer, wherein the second electrode comp ri ses: a second contact pad proximate the edge of the second nitride layer, a second probe at an edge of the outlet port, and a second lead connecting the second contact pad and the second probe.
The device of claim 1, wherein a second plurality of viewports is defined in the third nitride layer, further comprising: a second graphene sheet disposed on the third nitride layer covering the second plurality of viewports.
A device comprising: a first substrate, the first substrate having a first surface and a second surface; a first nitride layer disposed on the first surface of the first substrate and a second nitride layer disposed on the second surface of the first substrate; an oxide layer disposed on the second nitride layer; a third nitride layer disposed on the oxide layer; a cavity defined in the first nitride layer and the first substrate; a channel defined in the oxide layer; an inlet port and an outlet port defined in the third nitride layer in fluid communication with the channel; 22 Attorney Docket No.: 2014-129-02 a plurality of viewports defined in the third nitride layer positioned between the inlet port and the outlet port, at least some of the plurality of viewports positioned opposite the cavity; and a first graphene sheet disposed on the third nitride layer covering the plurality of viewports.
A method comprising: (a) forming a first oxide layer on a first surface of a first substrate and a second oxide layer on a second surface of the first substrate; (b) depositing a first nitride layer on the first oxide layer and a second nitride layer on the second oxide layer; (c) removing a portion of the first nitride layer and the first oxide layer; (d) forming a cavity in the first substrate to expose the second oxide layer; (e) depositing a third nitride layer on the first nitride layer, first substrate walls of the cavity, and the second oxide layer; (f) forming an inlet port, an outlet port, and a plurality of viewports between the inlet port and the outlet port in the second nitride layer, at least some of the plurality of viewports positioned to be opposite the cavity; (g) removing a portion of the second oxide layer to form a channel from the inlet port to the outlet port; and (h) positioning a graphene sheet on the second nitride layer to cover the plurality of viewports.
The method of claim 16, further comprising: forming a first oxide layer on a first surface of a second substrate and a second oxide layer on a second surface of the second substrate; depositing a first nitride layer on the first oxide layer of the second substrate and a second nitride layer on the second oxide layer of the second substrate; removing a portion of the first nitride layer and the first oxide layer of the second substrate; forming a cavity in the second substrate to expose the second oxide layer of the second substrate; 23 Attorney Docket No.: 2014-129-02 depositing a polymer material on the second nitride layer of the second substrate; removing a portion of the polymer material, the second nitride layer of the second substrate, and the second oxide layer of the second substrate to form a through hole; and joining the graphene sheet of the first substrate to the second nitride layer of the second substrate with the polymer material, wherein the cavity of the first substrate is aligned with the though hole of the second substrate.
The method of claim 16, further comprising: after operation (e), forming a first electrode on the second nitride layer, wherein the first electrode includes a first contact pad proximate an edge of the second nitride layer, a first probe at an edge of the inlet port, and a first lead connecting the first contact pad and the first probe; and forming a second electrode on the second nitride layer, wherein the second electrode includes a second contact pad proximate the edge of the second nitride layer, a second probe at an edge of the outlet port, and a second lead connecting the second contact pad and the second probe.
The method of claim 16, wherein operation (f) includes forming a second plurality of viewports in the third nitride layer.
Layer stacks claimed or described, ordered top of device to substrate.
liquid flow cell (graphene on nitride, two-plate)
Materials described outside the worked examples.
graphene
substrate
Additional fabrication and treatment steps described in the patent.
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Thickness | 60–500 nm | — |
Thickness |
Related documents with shared materials, methods, properties, or citations.
Patent
Atlas literature
Patent
US 9,449,787Patent drawings and their descriptions. Click a drawing to enlarge it.
Figure 1 shows an example of a flow diagram illustrating a manufacturing process for a liquid flow cell.
Figures 2A-2 I show examples of schematic illustrations of a liquid flow cell at various stages in the manufacturing process.
Figure 2J shows an example of a cross-sectional schematic illustration of a liquid flow cell.
Figure 3 shows an example of a flow diagram illustrating a manufacturing process for a liquid flow cell having a top plate.
Figures 4A-4G show examples of schematic illustrations of a liquid flow cell having a top plate at various stages in the manufacturing process.
Figure 5 shows an example of a top-down schematic illustration of a liquid flow cell including electrodes.
Figure 6 shows an example of a cross-sectional schematic illustration of a liquid flow cell including two graphene sheets.
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
A device comprising: a first plate, the first plate comprising: a first substrate, the first substrate having a first surface and a second surface; a first oxide layer disposed on the first surface of the first substrate and a second oxide layer disposed on the second surface of the first substrate; a first nitride layer disposed on the first oxide layer and a second nitride layer disposed on the second oxide layer; a cavity defined in the first oxide layer, the first nitride layer, and the first substrate, the cavity including a third nitride layer disposed on walls of the first substrate and the second oxide layer that define the cavity; a channel defined in the second oxide layer; an inlet port and an outlet port defined in the second nitride layer in fluid communication with the channel; a plurality of viewports defined in the second nitride layer positioned between the inlet port and the outlet port, at least some of the plurality of viewports positioned opposite the cavity; and a first graphene sheet disposed on the second nitride layer covering the plurality of viewports.
The device of claim 1, further comprising: a second plate, the second plate comprising: a second substrate having a first surface and a second surface; a third oxide layer disposed on the first surface of the second substrate and a fourth oxide layer disposed on the second surface of the second substrate; and a third nitride layer disposed on the third oxide layer and a fourth nitride layer disposed on the fourth oxide layer, wherein the second plate defines a through hole Attorney Docket No.: 2014-129-02 through the third nitride layer, the third oxide layer, the second substrate, the fourth oxide layer, and the fourth nitride layer; and a polymer material joining the graphene sheet of the first plate and the fourth nitride layer of the second plate, wherein the first and the second plates are joined so that the cavity of the first plate is aligned with the though hole in the second plate.
The device of claim 1, wherein first substrate comprises silicon, wherein the first and second oxide layers comprise silicon oxide, and wherein the first, second, and third nitride layers comprise silicon nitride.
The device of claim 1, wherein the graphene sheet comprises a few layers of graphene.
The device of claim 1, wherein the inlet port, the outlet port, and the plurality of view ports are about 60 nanometers to 500 nanometers in diameter.
The device of claim 1, wherein the first substrate is about 150 microns to 450 microns thick.
The device of claim 1, wherein the first surface and the second surface have dimensions of about 2 millimeters to 8 millimeters by about 2 millimeters to 8 millimeters. 21 Attorney Docket No.: 2014-129-02
The device of claim 1, further comprising: a first electrode disposed on the second nitride layer, wherein the first electrode comp ri ses: a first contact pad proximate an edge of the second nitride layer, a first probe at an edge of the inlet port, and a first lead connecting the first contact pad and the first probe; and a second electrode disposed on the second nitride layer, wherein the second electrode comp ri ses: a second contact pad proximate the edge of the second nitride layer, a second probe at an edge of the outlet port, and a second lead connecting the second contact pad and the second probe.
The device of claim 1, wherein a second plurality of viewports is defined in the third nitride layer, further comprising: a second graphene sheet disposed on the third nitride layer covering the second plurality of viewports.
A device comprising: a first substrate, the first substrate having a first surface and a second surface; a first nitride layer disposed on the first surface of the first substrate and a second nitride layer disposed on the second surface of the first substrate; an oxide layer disposed on the second nitride layer; a third nitride layer disposed on the oxide layer; a cavity defined in the first nitride layer and the first substrate; a channel defined in the oxide layer; an inlet port and an outlet port defined in the third nitride layer in fluid communication with the channel; 22 Attorney Docket No.: 2014-129-02 a plurality of viewports defined in the third nitride layer positioned between the inlet port and the outlet port, at least some of the plurality of viewports positioned opposite the cavity; and a first graphene sheet disposed on the third nitride layer covering the plurality of viewports.
A method comprising: (a) forming a first oxide layer on a first surface of a first substrate and a second oxide layer on a second surface of the first substrate; (b) depositing a first nitride layer on the first oxide layer and a second nitride layer on the second oxide layer; (c) removing a portion of the first nitride layer and the first oxide layer; (d) forming a cavity in the first substrate to expose the second oxide layer; (e) depositing a third nitride layer on the first nitride layer, first substrate walls of the cavity, and the second oxide layer; (f) forming an inlet port, an outlet port, and a plurality of viewports between the inlet port and the outlet port in the second nitride layer, at least some of the plurality of viewports positioned to be opposite the cavity; (g) removing a portion of the second oxide layer to form a channel from the inlet port to the outlet port; and (h) positioning a graphene sheet on the second nitride layer to cover the plurality of viewports.
The method of claim 16, further comprising: forming a first oxide layer on a first surface of a second substrate and a second oxide layer on a second surface of the second substrate; depositing a first nitride layer on the first oxide layer of the second substrate and a second nitride layer on the second oxide layer of the second substrate; removing a portion of the first nitride layer and the first oxide layer of the second substrate; forming a cavity in the second substrate to expose the second oxide layer of the second substrate; 23 Attorney Docket No.: 2014-129-02 depositing a polymer material on the second nitride layer of the second substrate; removing a portion of the polymer material, the second nitride layer of the second substrate, and the second oxide layer of the second substrate to form a through hole; and joining the graphene sheet of the first substrate to the second nitride layer of the second substrate with the polymer material, wherein the cavity of the first substrate is aligned with the though hole of the second substrate.
The method of claim 16, further comprising: after operation (e), forming a first electrode on the second nitride layer, wherein the first electrode includes a first contact pad proximate an edge of the second nitride layer, a first probe at an edge of the inlet port, and a first lead connecting the first contact pad and the first probe; and forming a second electrode on the second nitride layer, wherein the second electrode includes a second contact pad proximate the edge of the second nitride layer, a second probe at an edge of the outlet port, and a second lead connecting the second contact pad and the second probe.
The method of claim 16, wherein operation (f) includes forming a second plurality of viewports in the third nitride layer.
Layer stacks claimed or described, ordered top of device to substrate.
liquid flow cell (graphene on nitride, two-plate)
Materials described outside the worked examples.
graphene
substrate
Additional fabrication and treatment steps described in the patent.
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Thickness | 60–500 nm | — |
Thickness |
Related documents with shared materials, methods, properties, or citations.
Patent
Atlas literature
Patent
US 9,449,787Patent drawings and their descriptions. Click a drawing to enlarge it.
Figure 1 shows an example of a flow diagram illustrating a manufacturing process for a liquid flow cell.
Figures 2A-2 I show examples of schematic illustrations of a liquid flow cell at various stages in the manufacturing process.
Figure 2J shows an example of a cross-sectional schematic illustration of a liquid flow cell.
Figure 3 shows an example of a flow diagram illustrating a manufacturing process for a liquid flow cell having a top plate.
Figures 4A-4G show examples of schematic illustrations of a liquid flow cell having a top plate at various stages in the manufacturing process.
Figure 5 shows an example of a top-down schematic illustration of a liquid flow cell including electrodes.
Figure 6 shows an example of a cross-sectional schematic illustration of a liquid flow cell including two graphene sheets.
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
A device comprising: a first plate, the first plate comprising: a first substrate, the first substrate having a first surface and a second surface; a first oxide layer disposed on the first surface of the first substrate and a second oxide layer disposed on the second surface of the first substrate; a first nitride layer disposed on the first oxide layer and a second nitride layer disposed on the second oxide layer; a cavity defined in the first oxide layer, the first nitride layer, and the first substrate, the cavity including a third nitride layer disposed on walls of the first substrate and the second oxide layer that define the cavity; a channel defined in the second oxide layer; an inlet port and an outlet port defined in the second nitride layer in fluid communication with the channel; a plurality of viewports defined in the second nitride layer positioned between the inlet port and the outlet port, at least some of the plurality of viewports positioned opposite the cavity; and a first graphene sheet disposed on the second nitride layer covering the plurality of viewports.
The device of claim 1, further comprising: a second plate, the second plate comprising: a second substrate having a first surface and a second surface; a third oxide layer disposed on the first surface of the second substrate and a fourth oxide layer disposed on the second surface of the second substrate; and a third nitride layer disposed on the third oxide layer and a fourth nitride layer disposed on the fourth oxide layer, wherein the second plate defines a through hole Attorney Docket No.: 2014-129-02 through the third nitride layer, the third oxide layer, the second substrate, the fourth oxide layer, and the fourth nitride layer; and a polymer material joining the graphene sheet of the first plate and the fourth nitride layer of the second plate, wherein the first and the second plates are joined so that the cavity of the first plate is aligned with the though hole in the second plate.
The device of claim 1, wherein first substrate comprises silicon, wherein the first and second oxide layers comprise silicon oxide, and wherein the first, second, and third nitride layers comprise silicon nitride.
The device of claim 1, wherein the graphene sheet comprises a few layers of graphene.
The device of claim 1, wherein the inlet port, the outlet port, and the plurality of view ports are about 60 nanometers to 500 nanometers in diameter.
The device of claim 1, wherein the first substrate is about 150 microns to 450 microns thick.
The device of claim 1, wherein the first surface and the second surface have dimensions of about 2 millimeters to 8 millimeters by about 2 millimeters to 8 millimeters. 21 Attorney Docket No.: 2014-129-02
The device of claim 1, further comprising: a first electrode disposed on the second nitride layer, wherein the first electrode comp ri ses: a first contact pad proximate an edge of the second nitride layer, a first probe at an edge of the inlet port, and a first lead connecting the first contact pad and the first probe; and a second electrode disposed on the second nitride layer, wherein the second electrode comp ri ses: a second contact pad proximate the edge of the second nitride layer, a second probe at an edge of the outlet port, and a second lead connecting the second contact pad and the second probe.
The device of claim 1, wherein a second plurality of viewports is defined in the third nitride layer, further comprising: a second graphene sheet disposed on the third nitride layer covering the second plurality of viewports.
A device comprising: a first substrate, the first substrate having a first surface and a second surface; a first nitride layer disposed on the first surface of the first substrate and a second nitride layer disposed on the second surface of the first substrate; an oxide layer disposed on the second nitride layer; a third nitride layer disposed on the oxide layer; a cavity defined in the first nitride layer and the first substrate; a channel defined in the oxide layer; an inlet port and an outlet port defined in the third nitride layer in fluid communication with the channel; 22 Attorney Docket No.: 2014-129-02 a plurality of viewports defined in the third nitride layer positioned between the inlet port and the outlet port, at least some of the plurality of viewports positioned opposite the cavity; and a first graphene sheet disposed on the third nitride layer covering the plurality of viewports.
A method comprising: (a) forming a first oxide layer on a first surface of a first substrate and a second oxide layer on a second surface of the first substrate; (b) depositing a first nitride layer on the first oxide layer and a second nitride layer on the second oxide layer; (c) removing a portion of the first nitride layer and the first oxide layer; (d) forming a cavity in the first substrate to expose the second oxide layer; (e) depositing a third nitride layer on the first nitride layer, first substrate walls of the cavity, and the second oxide layer; (f) forming an inlet port, an outlet port, and a plurality of viewports between the inlet port and the outlet port in the second nitride layer, at least some of the plurality of viewports positioned to be opposite the cavity; (g) removing a portion of the second oxide layer to form a channel from the inlet port to the outlet port; and (h) positioning a graphene sheet on the second nitride layer to cover the plurality of viewports.
The method of claim 16, further comprising: forming a first oxide layer on a first surface of a second substrate and a second oxide layer on a second surface of the second substrate; depositing a first nitride layer on the first oxide layer of the second substrate and a second nitride layer on the second oxide layer of the second substrate; removing a portion of the first nitride layer and the first oxide layer of the second substrate; forming a cavity in the second substrate to expose the second oxide layer of the second substrate; 23 Attorney Docket No.: 2014-129-02 depositing a polymer material on the second nitride layer of the second substrate; removing a portion of the polymer material, the second nitride layer of the second substrate, and the second oxide layer of the second substrate to form a through hole; and joining the graphene sheet of the first substrate to the second nitride layer of the second substrate with the polymer material, wherein the cavity of the first substrate is aligned with the though hole of the second substrate.
The method of claim 16, further comprising: after operation (e), forming a first electrode on the second nitride layer, wherein the first electrode includes a first contact pad proximate an edge of the second nitride layer, a first probe at an edge of the inlet port, and a first lead connecting the first contact pad and the first probe; and forming a second electrode on the second nitride layer, wherein the second electrode includes a second contact pad proximate the edge of the second nitride layer, a second probe at an edge of the outlet port, and a second lead connecting the second contact pad and the second probe.
The method of claim 16, wherein operation (f) includes forming a second plurality of viewports in the third nitride layer.
Layer stacks claimed or described, ordered top of device to substrate.
liquid flow cell (graphene on nitride, two-plate)
Materials described outside the worked examples.
graphene
substrate
Additional fabrication and treatment steps described in the patent.
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Thickness | 60–500 nm | — |
Thickness |
Related documents with shared materials, methods, properties, or citations.
liquid flow cell (graphene on nitride, single substrate, alternate stack)
oxide layer
nitride layer
polymer material
silicon
Si
silicon oxide
SiO₂
silicon nitride
Si₃N₄
gold
Au
platinum
Pt
epoxy-based photoresist
| — |
Thickness | 2–8 mm | — |
Thickness | 50–300 nm | — |
Thickness | 20–60 nm | — |
Thickness | 200–500 µm | — |
Thickness | 60–120 nm | — |
Thickness | 80–100 nm | — |
Thickness | 250–1000 nm | — |
Thickness | 500–2000 nm | — |
Thickness | 50000–1500000 nm | — |
Thickness | 10–20 nm | — |
Thickness | 2–8 µm | — |
Thickness | 1–4 mm | — |
Thickness | 2–3 mm | — |
Temperature | 50–150 °C | — |
Duration | 5–25 minutes | — |
liquid flow cell (graphene on nitride, single substrate, alternate stack)
oxide layer
nitride layer
polymer material
silicon
Si
silicon oxide
SiO₂
silicon nitride
Si₃N₄
gold
Au
platinum
Pt
epoxy-based photoresist
| — |
Thickness | 2–8 mm | — |
Thickness | 50–300 nm | — |
Thickness | 20–60 nm | — |
Thickness | 200–500 µm | — |
Thickness | 60–120 nm | — |
Thickness | 80–100 nm | — |
Thickness | 250–1000 nm | — |
Thickness | 500–2000 nm | — |
Thickness | 50000–1500000 nm | — |
Thickness | 10–20 nm | — |
Thickness | 2–8 µm | — |
Thickness | 1–4 mm | — |
Thickness | 2–3 mm | — |
Temperature | 50–150 °C | — |
Duration | 5–25 minutes | — |
liquid flow cell (graphene on nitride, single substrate, alternate stack)
oxide layer
nitride layer
polymer material
silicon
Si
silicon oxide
SiO₂
silicon nitride
Si₃N₄
gold
Au
platinum
Pt
epoxy-based photoresist
| — |
Thickness | 2–8 mm | — |
Thickness | 50–300 nm | — |
Thickness | 20–60 nm | — |
Thickness | 200–500 µm | — |
Thickness | 60–120 nm | — |
Thickness | 80–100 nm | — |
Thickness | 250–1000 nm | — |
Thickness | 500–2000 nm | — |
Thickness | 50000–1500000 nm | — |
Thickness | 10–20 nm | — |
Thickness | 2–8 µm | — |
Thickness | 1–4 mm | — |
Thickness | 2–3 mm | — |
Temperature | 50–150 °C | — |
Duration | 5–25 minutes | — |
liquid flow cell (graphene on nitride, single substrate, alternate stack)
oxide layer
nitride layer
polymer material
silicon
Si
silicon oxide
SiO₂
silicon nitride
Si₃N₄
gold
Au
platinum
Pt
epoxy-based photoresist
| — |
Thickness | 2–8 mm | — |
Thickness | 50–300 nm | — |
Thickness | 20–60 nm | — |
Thickness | 200–500 µm | — |
Thickness | 60–120 nm | — |
Thickness | 80–100 nm | — |
Thickness | 250–1000 nm | — |
Thickness | 500–2000 nm | — |
Thickness | 50000–1500000 nm | — |
Thickness | 10–20 nm | — |
Thickness | 2–8 µm | — |
Thickness | 1–4 mm | — |
Thickness | 2–3 mm | — |
Temperature | 50–150 °C | — |
Duration | 5–25 minutes | — |