Method for preparing thin GaN layers by implantation and recycling of a starting substrate | Matter42 Literature
Patent
Atlas literature
Patent
US 8,778,775
Method for preparing thin GaN layers by implantation and recycling of a starting substrate
Aurélie Tauzin
US
Claims
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
3 independent · 23 dependent
1
IndependentGaNHe+H+
A method of fabrication of a thin layer of GaN from a starting substrate of which at least a thick surface area along a free face of the starting substrate comprises GaN, the method comprising the following steps: bombarding the free face of the starting substrate with helium ions and hydrogen ions, wherein the helium ions are implanted first in the thick surface area and the hydrogen ions are implanted second, and wherein implantation doses of the helium ions and the hydrogen ions each range between 1.10 7 atoms/cm2 and 4.10 17 atoms/cm2; and applying a fracture treatment to the starting substrate adapted to cause a detachment of the thick surface area between the free face and an implantation depth of the helium ions and of the hydrogen ions from a remainder of the starting substrate.
2
Dependent← claim 1He+H+
The method according to claim 1, wherein the implantation dose of the helium ions is at least equal to the implantation dose of the hydrogen ions.
3
Dependent← claim 1GaN
The method according to claim 1 or claim 2, further comprising recycling the remainder of the starting substrate after applying the fracture treatment.
5
Dependent← claim 1GaN
The method according to claim 1, further comprising bringing the starting substrate into intimate contact with a host substrate via the free -2- BR₁NK S......... i&tL f3Ni App. Ser. No. 12/51 8,198 Response to Office Action of Reply dated face before applying the fracture treatment.
19
Dependent← claim 1He+
The method according to claim 1, wherein helium ion implantation dose ranges between 1.10 7 and 2.10 17 He +/cm2.
20
Dependent← claim 1H+
The method according to claim 1, wherein the hydrogen ion implantation dose ranges between 1.10 7 and 2.10 17 H+/cm2.
21
Dependent← claim 1
The method according to claim 1, wherein a -4- BR₁NK S......... i&tL f3Ni App. Ser. No. 12/51 8,198 Response to Office Action of Reply dated cumulative implantation dose is between approximately cm2.
22
Dependent← claim 1
The method according to claim 1, wherein an implantation is greater than an implantation energy
23
Dependent← claim 1
The method according to claim 1, wherein an between 90 keV and 210 keV and an implantation and 120 keV.
24
Dependent← claim 1
The method according to claim 1, further perfecting the detachment of all the thin layer,
25
Independent
- 26. -5- R K......... i&tL f3Ni canceled
26
Independent
canceled 3.10 7 atoms/cm 2 and 4.5 10 17 atoms/implantation energy of the helium ion of the hydrogen ion implantation. implantation energy of the helium ions is energy of the hydrogen ions is between 60 keV comprising applying a finishing heat treatment for including in any non-bonded areas.
Materials
Materials described outside the worked examples.
GaN
Thin Layer Substrate Material
helium ions
He+
Process steps
Additional fabrication and treatment steps described in the patent.
1
Ion Implantation
Step 1
Process details
species order:helium first, hydrogen second
helium dose range:1e7 to 4e17 atoms/cm2
hydrogen dose range:1e7 to 4e17 atoms/cm2
helium energy range keV:90 to 210
hydrogen energy range keV:
Reported properties
Performance values and ranges asserted in the specification or claims.
Property
Value
Material
Thickness
≤ 1 µm
—
Why these are connected
Related documents with shared materials, methods, properties, or citations.
Method for preparing thin GaN layers by implantation and recycling of a starting substrate
Aurélie Tauzin
US
Claims
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
3 independent · 23 dependent
1
IndependentGaNHe+H+
A method of fabrication of a thin layer of GaN from a starting substrate of which at least a thick surface area along a free face of the starting substrate comprises GaN, the method comprising the following steps: bombarding the free face of the starting substrate with helium ions and hydrogen ions, wherein the helium ions are implanted first in the thick surface area and the hydrogen ions are implanted second, and wherein implantation doses of the helium ions and the hydrogen ions each range between 1.10 7 atoms/cm2 and 4.10 17 atoms/cm2; and applying a fracture treatment to the starting substrate adapted to cause a detachment of the thick surface area between the free face and an implantation depth of the helium ions and of the hydrogen ions from a remainder of the starting substrate.
2
Dependent← claim 1He+H+
The method according to claim 1, wherein the implantation dose of the helium ions is at least equal to the implantation dose of the hydrogen ions.
3
Dependent← claim 1GaN
The method according to claim 1 or claim 2, further comprising recycling the remainder of the starting substrate after applying the fracture treatment.
5
Dependent← claim 1GaN
The method according to claim 1, further comprising bringing the starting substrate into intimate contact with a host substrate via the free -2- BR₁NK S......... i&tL f3Ni App. Ser. No. 12/51 8,198 Response to Office Action of Reply dated face before applying the fracture treatment.
19
Dependent← claim 1He+
The method according to claim 1, wherein helium ion implantation dose ranges between 1.10 7 and 2.10 17 He +/cm2.
20
Dependent← claim 1H+
The method according to claim 1, wherein the hydrogen ion implantation dose ranges between 1.10 7 and 2.10 17 H+/cm2.
21
Dependent← claim 1
The method according to claim 1, wherein a -4- BR₁NK S......... i&tL f3Ni App. Ser. No. 12/51 8,198 Response to Office Action of Reply dated cumulative implantation dose is between approximately cm2.
22
Dependent← claim 1
The method according to claim 1, wherein an implantation is greater than an implantation energy
23
Dependent← claim 1
The method according to claim 1, wherein an between 90 keV and 210 keV and an implantation and 120 keV.
24
Dependent← claim 1
The method according to claim 1, further perfecting the detachment of all the thin layer,
25
Independent
- 26. -5- R K......... i&tL f3Ni canceled
26
Independent
canceled 3.10 7 atoms/cm 2 and 4.5 10 17 atoms/implantation energy of the helium ion of the hydrogen ion implantation. implantation energy of the helium ions is energy of the hydrogen ions is between 60 keV comprising applying a finishing heat treatment for including in any non-bonded areas.
Materials
Materials described outside the worked examples.
GaN
Thin Layer Substrate Material
helium ions
He+
Process steps
Additional fabrication and treatment steps described in the patent.
1
Ion Implantation
Step 1
Process details
species order:helium first, hydrogen second
helium dose range:1e7 to 4e17 atoms/cm2
hydrogen dose range:1e7 to 4e17 atoms/cm2
helium energy range keV:90 to 210
hydrogen energy range keV:
Reported properties
Performance values and ranges asserted in the specification or claims.
Property
Value
Material
Thickness
≤ 1 µm
—
Why these are connected
Related documents with shared materials, methods, properties, or citations.
Method for preparing thin GaN layers by implantation and recycling of a starting substrate
Aurélie Tauzin
US
Claims
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
3 independent · 23 dependent
1
IndependentGaNHe+H+
A method of fabrication of a thin layer of GaN from a starting substrate of which at least a thick surface area along a free face of the starting substrate comprises GaN, the method comprising the following steps: bombarding the free face of the starting substrate with helium ions and hydrogen ions, wherein the helium ions are implanted first in the thick surface area and the hydrogen ions are implanted second, and wherein implantation doses of the helium ions and the hydrogen ions each range between 1.10 7 atoms/cm2 and 4.10 17 atoms/cm2; and applying a fracture treatment to the starting substrate adapted to cause a detachment of the thick surface area between the free face and an implantation depth of the helium ions and of the hydrogen ions from a remainder of the starting substrate.
2
Dependent← claim 1He+H+
The method according to claim 1, wherein the implantation dose of the helium ions is at least equal to the implantation dose of the hydrogen ions.
3
Dependent← claim 1GaN
The method according to claim 1 or claim 2, further comprising recycling the remainder of the starting substrate after applying the fracture treatment.
5
Dependent← claim 1GaN
The method according to claim 1, further comprising bringing the starting substrate into intimate contact with a host substrate via the free -2- BR₁NK S......... i&tL f3Ni App. Ser. No. 12/51 8,198 Response to Office Action of Reply dated face before applying the fracture treatment.
19
Dependent← claim 1He+
The method according to claim 1, wherein helium ion implantation dose ranges between 1.10 7 and 2.10 17 He +/cm2.
20
Dependent← claim 1H+
The method according to claim 1, wherein the hydrogen ion implantation dose ranges between 1.10 7 and 2.10 17 H+/cm2.
21
Dependent← claim 1
The method according to claim 1, wherein a -4- BR₁NK S......... i&tL f3Ni App. Ser. No. 12/51 8,198 Response to Office Action of Reply dated cumulative implantation dose is between approximately cm2.
22
Dependent← claim 1
The method according to claim 1, wherein an implantation is greater than an implantation energy
23
Dependent← claim 1
The method according to claim 1, wherein an between 90 keV and 210 keV and an implantation and 120 keV.
24
Dependent← claim 1
The method according to claim 1, further perfecting the detachment of all the thin layer,
25
Independent
- 26. -5- R K......... i&tL f3Ni canceled
26
Independent
canceled 3.10 7 atoms/cm 2 and 4.5 10 17 atoms/implantation energy of the helium ion of the hydrogen ion implantation. implantation energy of the helium ions is energy of the hydrogen ions is between 60 keV comprising applying a finishing heat treatment for including in any non-bonded areas.
Materials
Materials described outside the worked examples.
GaN
Thin Layer Substrate Material
helium ions
He+
Process steps
Additional fabrication and treatment steps described in the patent.
1
Ion Implantation
Step 1
Process details
species order:helium first, hydrogen second
helium dose range:1e7 to 4e17 atoms/cm2
hydrogen dose range:1e7 to 4e17 atoms/cm2
helium energy range keV:90 to 210
hydrogen energy range keV:
Reported properties
Performance values and ranges asserted in the specification or claims.
Property
Value
Material
Thickness
≤ 1 µm
—
Why these are connected
Related documents with shared materials, methods, properties, or citations.
Method for preparing thin GaN layers by implantation and recycling of a starting substrate
Aurélie Tauzin
US
Claims
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
3 independent · 23 dependent
1
IndependentGaNHe+H+
A method of fabrication of a thin layer of GaN from a starting substrate of which at least a thick surface area along a free face of the starting substrate comprises GaN, the method comprising the following steps: bombarding the free face of the starting substrate with helium ions and hydrogen ions, wherein the helium ions are implanted first in the thick surface area and the hydrogen ions are implanted second, and wherein implantation doses of the helium ions and the hydrogen ions each range between 1.10 7 atoms/cm2 and 4.10 17 atoms/cm2; and applying a fracture treatment to the starting substrate adapted to cause a detachment of the thick surface area between the free face and an implantation depth of the helium ions and of the hydrogen ions from a remainder of the starting substrate.
2
Dependent← claim 1He+H+
The method according to claim 1, wherein the implantation dose of the helium ions is at least equal to the implantation dose of the hydrogen ions.
3
Dependent← claim 1GaN
The method according to claim 1 or claim 2, further comprising recycling the remainder of the starting substrate after applying the fracture treatment.
5
Dependent← claim 1GaN
The method according to claim 1, further comprising bringing the starting substrate into intimate contact with a host substrate via the free -2- BR₁NK S......... i&tL f3Ni App. Ser. No. 12/51 8,198 Response to Office Action of Reply dated face before applying the fracture treatment.
19
Dependent← claim 1He+
The method according to claim 1, wherein helium ion implantation dose ranges between 1.10 7 and 2.10 17 He +/cm2.
20
Dependent← claim 1H+
The method according to claim 1, wherein the hydrogen ion implantation dose ranges between 1.10 7 and 2.10 17 H+/cm2.
21
Dependent← claim 1
The method according to claim 1, wherein a -4- BR₁NK S......... i&tL f3Ni App. Ser. No. 12/51 8,198 Response to Office Action of Reply dated cumulative implantation dose is between approximately cm2.
22
Dependent← claim 1
The method according to claim 1, wherein an implantation is greater than an implantation energy
23
Dependent← claim 1
The method according to claim 1, wherein an between 90 keV and 210 keV and an implantation and 120 keV.
24
Dependent← claim 1
The method according to claim 1, further perfecting the detachment of all the thin layer,
25
Independent
- 26. -5- R K......... i&tL f3Ni canceled
26
Independent
canceled 3.10 7 atoms/cm 2 and 4.5 10 17 atoms/implantation energy of the helium ion of the hydrogen ion implantation. implantation energy of the helium ions is energy of the hydrogen ions is between 60 keV comprising applying a finishing heat treatment for including in any non-bonded areas.
Materials
Materials described outside the worked examples.
GaN
Thin Layer Substrate Material
helium ions
He+
Process steps
Additional fabrication and treatment steps described in the patent.
1
Ion Implantation
Step 1
Process details
species order:helium first, hydrogen second
helium dose range:1e7 to 4e17 atoms/cm2
hydrogen dose range:1e7 to 4e17 atoms/cm2
helium energy range keV:90 to 210
hydrogen energy range keV:
Reported properties
Performance values and ranges asserted in the specification or claims.
Property
Value
Material
Thickness
≤ 1 µm
—
Why these are connected
Related documents with shared materials, methods, properties, or citations.
description:Fracture treatment to detach thin GaN layer at implantation depth; may include heat treatment and/or mechanical stresses, ultrasound, microwaves
Materials:GaN
3
Embrittlement Heat Treatment
Step 3
Temperature
400°C
Process details
description:Embrittlement treatment before bonding to host substrate; heat treatment corresponding to at least 85% of fracture thermo-mechanical budget
max temperature c:400
thermo mechanical budget fraction:at least 85% (claim 8), at least 95% (claim 12)
Materials:GaN
4
Residual Fracture Treatment
Step 4
Temperature
250°C
Process details
description:Residual fracture treatment applied after bonding to host substrate; heat treatment at most 250°C or mechanical stresses at room temperature, ultrasound, or microwaves
max temperature c:250
temperature c upper bound:250
Materials:GaN
5
Polishing
Step 5
Process details
description:Optional preparation of remainder of starting substrate before recycling; at most one polishing of at most 1 micron thickness
description:Fracture treatment to detach thin GaN layer at implantation depth; may include heat treatment and/or mechanical stresses, ultrasound, microwaves
Materials:GaN
3
Embrittlement Heat Treatment
Step 3
Temperature
400°C
Process details
description:Embrittlement treatment before bonding to host substrate; heat treatment corresponding to at least 85% of fracture thermo-mechanical budget
max temperature c:400
thermo mechanical budget fraction:at least 85% (claim 8), at least 95% (claim 12)
Materials:GaN
4
Residual Fracture Treatment
Step 4
Temperature
250°C
Process details
description:Residual fracture treatment applied after bonding to host substrate; heat treatment at most 250°C or mechanical stresses at room temperature, ultrasound, or microwaves
max temperature c:250
temperature c upper bound:250
Materials:GaN
5
Polishing
Step 5
Process details
description:Optional preparation of remainder of starting substrate before recycling; at most one polishing of at most 1 micron thickness
description:Fracture treatment to detach thin GaN layer at implantation depth; may include heat treatment and/or mechanical stresses, ultrasound, microwaves
Materials:GaN
3
Embrittlement Heat Treatment
Step 3
Temperature
400°C
Process details
description:Embrittlement treatment before bonding to host substrate; heat treatment corresponding to at least 85% of fracture thermo-mechanical budget
max temperature c:400
thermo mechanical budget fraction:at least 85% (claim 8), at least 95% (claim 12)
Materials:GaN
4
Residual Fracture Treatment
Step 4
Temperature
250°C
Process details
description:Residual fracture treatment applied after bonding to host substrate; heat treatment at most 250°C or mechanical stresses at room temperature, ultrasound, or microwaves
max temperature c:250
temperature c upper bound:250
Materials:GaN
5
Polishing
Step 5
Process details
description:Optional preparation of remainder of starting substrate before recycling; at most one polishing of at most 1 micron thickness
description:Fracture treatment to detach thin GaN layer at implantation depth; may include heat treatment and/or mechanical stresses, ultrasound, microwaves
Materials:GaN
3
Embrittlement Heat Treatment
Step 3
Temperature
400°C
Process details
description:Embrittlement treatment before bonding to host substrate; heat treatment corresponding to at least 85% of fracture thermo-mechanical budget
max temperature c:400
thermo mechanical budget fraction:at least 85% (claim 8), at least 95% (claim 12)
Materials:GaN
4
Residual Fracture Treatment
Step 4
Temperature
250°C
Process details
description:Residual fracture treatment applied after bonding to host substrate; heat treatment at most 250°C or mechanical stresses at room temperature, ultrasound, or microwaves
max temperature c:250
temperature c upper bound:250
Materials:GaN
5
Polishing
Step 5
Process details
description:Optional preparation of remainder of starting substrate before recycling; at most one polishing of at most 1 micron thickness